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LECTURE NOTES : text: Skoog, Holler, Crouch, Principles of Instrumental Analysis, 6th Ed
(notes revised 2009)
1. Introduction to Lead Lab Lecture ppt 1
Critical Reviews in Anal. Chem.268-9
2. Statistics Lecture ppt
Reading: Introduction to Statistics.ppt
Text Chapter 1
3. Filtering and Massaging the Data. ppt
Reading: Signal and Noise Filtering
Text Chapters 2 &5
Instructions Deconvoluting UV-Vis
4. Chemistry of Lead Lecture ppt
Critical Reviews in Anal. Chem.269-285
5. Electrochemistry A: ISE ppt
TEXT Chapters 22 23
6. Really Basic Optics ppt
Text Chapters 6&7
7. Beer's Laws and It's Implications ppt
Text Chapter 13
8. UV-Vis Spectroscopies ppt
Text Chapters 8&9; 14, 15, and 18
9. IR and NMR spectroscopies ppt
Text Chapters 16,17,19
see this great website
10. GC-MS ppt
Text Chapters 26, 27, and 20
11. Standard Operating Procedures
LEAD LABORATORIES
** indicates revised Spring 2009)
Anal Chem Article on Team Work
1 : Calibrate Your Writing
GFAA Group A Version 1
GFAA Group A Version 2
GFAA Group E Version 1
GFAA Group E Version 2
ICPMS Group B
ICPMS Group C
ICPMS Group D
2**: Population Analysis
Needleman New Eng. J. Med, 1979.
Ernhardt Ethics & Behavior 1993
Needleman Ethics & Behavior 1993
Scarr Ethics & Behavior 1993
Needleman New Eng J Med 1990
3**: S/N and filtering
4**: PbS ion selective electrode
Kamata et al Anal. Chem. 1991
5 : IR study of Lead-EDTA chelate
6: **Chelation by Dithizone, UV-Vis
Irving et al Anal Chim Acta 1969
7 . **Fluorescence Quenching of CB by Pb
8 : Atomic Absorption, Graphite Furnace
Creed et al Env. Sci. Tech. 1992
Marquardt et al Anal. Chem. 1996
9 : Anodic Stripping Voltammetry
Liu et al Anal. Chem. 1997
Zelic et al Electrochem Acta 1990
Feldman et al Anal. Chem. 1994
10: NMR of 207Pb-EDTA complex
11: Lead by lead sulphide (turbidity)
12: Lead by lead chromate (gravimetric)
13: Commercial spot tests
14: Electrolytic deposition of PbO2
15: Titrametric, EDTA with Eriochrome
16: Titrametric, EDTA, UV-Vis detection
17: Lead Iodide determination
18**: Stability of Dithizone by CV
Tomcsanyi Anal Chim Acta 1977
Kassim Inorg Chim Acta 1978
19Fluorescence of protoporphyrin
Hammond et al Env. Research 1985
20: ICP-MS determination of Pb isotopes
21: Preparative Chromatography for Lead
Manton et al Chem Geol 1988
22: Ion Pair HPLC of Lead EDTA
Shijo et al Anal. Sci. 1993
Liu et al J. Chromatography A 1998
23: GC of Tetraethyl Lead
Brunelto Atomic Spectroscopy 1992
24:** Hot Plate Acid Digestions
25: Sequential Soil Extractions
26: Soil Sampling
27: House Dust Sampling: Wet Wipe
28: House Dust Sampling: Vacuum
29: Water Sampling
30: Blood Sampling
31. Hand Dust Sampling
32. Community Based Problem Solving
Markkula Center for Ethics
33. The Johnson Controls Case
U.S. District Court
U.S. Supreme Court
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Raymond Lully, 1235 A.D.
Take two to three pounds of the juice of the Lunaria, add a solution of lead, alum, salpetre, sal ammoniac, silver-litharge, quick-silver sublimate, vinegar and ginger, then distil and calcinate. This powder is then thickened with a silver solution into paste. One part in a hundred of this paste, heated on a copper plate, could theoretically turn tin, lead, or quicksilver into silver at a ratio of one to a hundred parts.
RESOURCE DOCUMENTS
Critical Reviews in Anal. Chem.
Lead Analysis: Past and Present
Sublime Lead: A Biography of a 5000 Year Toxic Love Affair
cosmetic analysis literature search 1
cosmetic analysis literature search 2
cosmetic analysis literature search 3
Excel Sheets
Exam 1 Take Home 2009
ExamII Take Home 2009 Excel
ExamII Take Home 2009 word
1. Needleman Data
2. Boxcar Filtering Data
3. FFT Filtering
4. Deconvolution of UV-Vis peaks
5. XRF data April 1
6.
7.
8.
9.
Old Exams
1. 2008 Exam 1
Raw Data
1. 2008 ISE data
2. 2008 UV-Vis data
3. 2009 FAA data
4.
5.
9.
List of Instruments Used/Skills Acquired
2009 (for the resume)